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RAS PresidiumДоклады Российской академии наук. Химия, науки о материалах Doklady Chemistry

  • ISSN (Print) 2686-9535
  • ISSN (Online) 3034-5111

Preparation of copper and nickel based nanoparticles by magnetron sputtering and their use in sulfur–sulfur bond activation reaction

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PII
10.31857/S2686953524050022-1
DOI
10.31857/S2686953524050022
Publication type
Article
Status
Published
Authors
А. S. Kashin
  • Affiliation: N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
Volume/ Edition
Volume 518 / Issue number 1
Pages
23-31
Abstract
The present work is devoted to a systematic study of the advantages and limitations of the magnetron sputtering method, which is a convenient and promising way to obtain nanosized particles directly from the bulk metal, when it is used to prepare nanoparticles of the first-row transition metals. In the course of the study, variation of sputtering media based on ionic liquids, eutectic solvents, low and high molecular weight organic compounds was carried out. Particles of copper, nickel, a copper-nickel alloy and a copper-zinc alloy were obtained. Using the example of the activation reaction of the sulfur–sulfur bond in diphenyl disulfide, it has been shown that up to 96% of the sputtered copper can be effectively used in catalysis, whereas in the case of nickel and zinc about three quarters of the metal can be converted to an inactive form, at the same time readily oxidizable components can act as sacrificial stabilizers for moderately active metal particles in sputtering two-component alloys.
Keywords
наночастицы металлов тиоляты металлов магнетронное распыление электронная микроскопия ионные жидкости
Date of publication
18.09.2025
Year of publication
2025
Number of purchasers
0
Views
6

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